JWGB Instruments - https://english.jwgb.net Fri, 22 Dec 2023 03:38:38 +0000 en-US hourly 1 Surface DX400 https://english.jwgb.net/surface-dx400.html https://english.jwgb.net/surface-dx400.html#respond Thu, 21 Dec 2023 07:59:14 +0000 https://english.jwgb.net/?p=479

Outline

The Altamira DX 400 is the latest surface area analyzer based on the principle of dynamic chromatographic analysis. It achieves rapid determination of BET specific surface area, surpassing traditional products in terms of both accuracy and speed. Accuracy: It can accurately test standard samples with ultra-small specific surface area of 0.1 m2/g, with an accuracy of 0.01 m2/g. Speed: The testing speed is 3 times faster than traditional products, achieving ultra-high testing efficiency of 28 samples in 1 hour. Suitable for testing the positive and negative electrode materials of lithium cobalt oxide, ternary materials, lithium iron phosphate, graphite, silicon carbide and other small specific surface area samples.

Distinctive

  • The unique Dtech technology integrates Dstable stable testing technology, Dcal automatic calibration technology, Dtrap precise testing technology, Dsignal efficient testing technology, and Dctrl anti-blowing control technology, contributed to the high testing efficiency of the DX 400 series. The repeatability, stability, accuracy, and parallelism of the test results all reach the industry-leading level, especially for samples with a specific surface area less than 1 m2/g.
  • Dstable stable testing technology
  • The unique Dstable stable testing technology is adopted to ensure that the TCD signal is not affected by the liquid nitrogen level changes during the instrument testing process, ensuring the repeatability of the test results.
  • Dctrl anti-blowing control technology
  • The exclusive Dctrl Anti-blowing control technology is used to prevent instrument airway pollution caused by samples being blown away during testing, protect the safe operation of the instrument, and prolong the instrument's lifespan.
  • Dcal automatic calibration technology
  • The Dcal automatic calibration technology is adopted to ensure that the aging of the TCD filament during the instrument's lifecycle does not affect the test results, thus ensuring the stability of the test results throughout the instrument's lifecycle.
  • Dsignal efficient testing technology
  • The unique Dsignal efficient testing technology is adopted to achieve efficient completion of single-point BET test results within 7 minutes, and the testing efficiency can reach up to 4 samples tested in 7 minutes.
  • Dtrap precise testing technology
  • Dtrap precise testing technology The unique Dtrap precise testing technology is adopted to ensure that the control accuracy of the TCD signal during the testing process reaches 0.1mV, and is not affected by the environment, thus ensuring the accuracy of the test results.

Software

  • ☆ Testing Result Real-Time Calculation
    ☆ Real-time recording and storage of instrument control process
  • Datasheet
  • The newly developed DX 400 control software is an intelligent software that implements operation control, data acquisition, calculation analysis, and report preview on the Windows platform.

Analysis

  • Repeatability of BET specific surface area <1%
  • Samples Times Value(m2/g) Average (m2/g) Repeatability (%)
    Carbon black G9 1 9.164 9.19 0.31%
    2 9.222
    3 9.213
    4 9.158
    5 9.162
    6 9.218
    Graphite 1 1.8397 1.845 0.24%
    2 1.8462
    3 1.8482
    4 1.8518
    5 1.8467
    6 1.8393
  • Stability of BET specific surface area <1%
  • Samples Test time (days) Value(m2/g) Average (m2/g) Repeatability (%)
    Carbon black G9 1 9.168 0.186 0.26%
    3 9.213
    7 9.208
    15 9.158
    30 9.162
    60 9.208
  • Reach repeatability 0.01 m2/g,when testing samples with an ultra-small specific surface area of 0.1 m2/g
  • Samples Times Value(m2/g) Average (m2/g) Repeatability (%)
    Cathode material 1 0.1235 0.122 0.0033
    2 0.1189
    3 0.1251
    4 0.1159
    5 0.1242
    6 0.1228
  • Parallelism of BET specific surface area <1%
  • Samples By different equipment Value(m2/g) Average(m2/g) Repeatability(%)
    Carbon black G9 no.1 9.156 9.183 0.28%
    no.2 9.163
    no.3 9.213
    no.4 9.158
    no.5 9.192
    no.6 9.218

Specification

Model DX400series
Testing Theory Low-temperature nitrogen adsorption in flow chromatography
Testing function Single-point BET specific surface area testing
Testing Gas High-purity (99.999%) nitrogen-helium gas mixture 3:7 or 2:8
Detector Thermal conductivity detector with accuracy up to 0.1mV
SSA range >0.01 m2/g, standard sample testing repeatability ≤ 1%, parallelism ≤ 1%
Analysis Station Testing 4 samples at the same time
Size Length 700mm × Width 410mm × Height 785mm, weight approximately 30 Kg.
Environment temperature 15-35℃
Environment moisture 20%-80% humidity in an environment without condensation.
Electricity 100-240VAC,50/60Hz,Max power 200W
Recommend material Battery electrode materials such as lithium iron phosphate, ternary, graphite, lithium cobalt, oxide, lithium manganese oxide, etc.
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Sync 400 https://english.jwgb.net/sync-400.html https://english.jwgb.net/sync-400.html#respond Thu, 21 Dec 2023 07:58:04 +0000 https://english.jwgb.net/?p=477

Outline

Sync series, specific surface area and pore size analyzers, are the latest instruments to characterize the surface properties and pore structure of micro-nano materials, introduced by Beijing JWGB. The most common and reliable static-volumetric gas adsorption method is used in Sync series to analyze the adsorption behavior of materials. During the test, samples share the same Dewar and the same gas source, ensuring the accuracy and repeatability of the analysis test, and truly achieve no differential analysis between multiple stations.

Technical

  • Unique Vtech technology, including Vspacecold free space control technology, Vlevel¬ liquid nitrogen level control technology, Vstable stability test technology, and Vctrl powder elutriation control technology. further enhances the test efficiency of product on Sync, guarantees the more repeatable and stable test results, and can better meet the test requirements of macroporous materials.
  • Vctrl
  • Powder elutriation control technology The combination of software and hardware prevents the loss of sample out of sample cell, guarantees the test efficiency, avoids the contamination of the instrument gas path caused by the sample elutriation during the test, and protects the safety of the instrument operation.
  • Vspace
  • Cold free space control technology Vspace technology ensures that the cold free space of the entire system does not change during the test, and guarantees the accuracy, repeatability, and stability of the analysis results.
  • Vstable
  • Stability test technology Unique Vstable technology ensures the stability and accuracy of the test, so that the analysis accuracy of macroporous materials such as white carbon black and alumina is higher, the repeatability and stability are better, and the pore size analysis of materials above 50nm is truly realized.
  • Vlevel
  • Liquid nitrogen level control technology Based on their blowing process, the self-developed large capacity glass Dewar is different from the ordinary glass Dewar. it is made by independent research and development process and is composed of special material. It overcomes the defect of uneven thickness caused by blowing and is not fragile. It can guarantee a high vacuum for a long time, and has a long service life and safe properties.

Features

  • High test efficiency
  • Up to four samples can be analyzed simultaneously, so that the BET specific surface area test efficiency is up to 20min /sample, meeting the requirements of customers with large test requirements in the fields of production and scientific research.
  • Security
  • To ensure the safety of users, (1) Independently-operated safety protection software can remotely monitor the operating status of the instrument. When the instrument appears abnormal pressure or other dangers, it can automatically control the instrument, remove the abnormal danger situation and protect the safety of the instrument and the operator. (2) The protecting casing of the Dewar prevents the danger of splashing of low temperature liquid such as liquid nitrogen during the operation of the instrument.
  • Real time Monitoring of P0
  • Configure an independent P0 sensor to realize real-time monitoring of p0 during the test and eliminate the influence of ambient temperature and atmospheric pressure on the experimental results.
  • Multi-channel intake
  • The user can choose the multi-channel gas intake option, which is convenient for the user to switch freely of various adsorbed gases.
  • Visual display of operating status
  • A status display system equipped on the front panel of the instrument shows the working diagram of the instrument. The LED lamp of each valve on the display system is used to indicate the on-off of the electromagnetic valve. And the operating process of the instrument can be intuitively observed during the test process.
  • Linkable and remote access
  • The communication interface of the instrument is a LAN port, which can realize the integrated control of a computer as a host computer, and can remotely access and control the host computer.
  • Independent vacuum degasser
  • Standard configuration with a completely independent vacuum degasser can prepare the sample by programmable temperature. It is more intelligent, flexible, and convenient for sample pretreatment, and at the same time reduces the time caused by in-situ degassing on the analysis position, significantly improving test efficiency.
  • cryo Tune (Option)
  • Users can choose cryo Tune— a low-temperature cold bath system. Sync software has cryo Tune compatible setting, which is convenient for users to test adsorption isotherms at different temperatures.

Software

Real-time monitoring
  • Pressure balance
  • The unique adsorption equilibrium pressure intelligent judgment and control method is adopted. Under the condition of sufficient adsorption balance, the test efficiency is much higher than that of the fixed-point method. The software has an independent interface to display the adsorption equilibrium process of each sample in real time. This can help to understand the adsorption characteristics of the sample in real time, analyze the abnormal phenomena such as gas leakage and unsufficient pretreatment during the sample adsorption process, and monitor the operation of the instrument during the experiment.
  • Datasheet
  • Adsorption isotherm
  • The software has an independent interface to display the adsorption isotherms of each sample in real time, show the experiment progress and adsorption results in real time, helping to determine the experimental abnormalities such as air leakage and cold free space changes.
  • Datasheet
  • Manual control
  • Different from other manual on / off valve control, Sync software provides a series of combined automatic control processes, which facilitates users to perform manual operations for multiple purposes, greatly reducing the probability of manual operations failures. During the test, users can visually observe the pressure changes and valve status of various parts inside the instrument, which is convenient for users to understand the test process, and at the same time it is convenient for engineers to diagnose and maintain remotely.
    The software provides an automatic process of adding liquid nitrogen. After a long time of experiment, the user can safely add liquid nitrogen according to the prompt of software. The test process is automatically suspended and resumed during the period without human judgment, and the degree of automation is high.
  • Datasheet
  • Real-time record storage of instrument control process
  • Message window can be switched to display, can record experimental control process and software manual operation information of the instrument in real time, which is benefit for engineers to analyze and remotely diagnose abnormal data.
  • Datasheet
Data analysis
  • The physical adsorption calculation model includes:
  • -Isothermal absorption and desorption curve;
    -BET specific surface area (single point, multiple points);
    -Langmuir surface area;
    -Statistical thickness surface area. (STSA);
    -BJH pore size analysis;
    -t-plot analysis;
    -HK pore size analysis;
    -SF pore size analysis;
    -NLDFT pore size distribution;
    -Most acceptable pore size, Average pore size,
    Total pore volume;
    -Adsorption curve etc.;
  • Typical analysis example
  • Repeatability of specific
    surface area BET
    ≤1%
  • Sample Test number measurement Average Repeatability
    G8 1 9.094 9.17 0.66%
    2 9.222
    3 9.243
    4 9.098
    5 9.162
    6 9.228
    C8 1 127.367 126.6 0.31%
    2 126.362
    3 126.482
    4 126.578
    5 126.167
    6 126.863
  • Datasheet
  • Datasheet
  • Datasheet
  • Datasheet

Specification

Model Sync series
Test principle Static volumetric gas adsorption
Adsorbate gas N2、Ar、Kr、H2、O2、CO2、CO、NH3、CH4等非腐蚀性气体
Analysis port 1-4 samples tested at the same time
Pressure sensor 1000torr
P/P0 range 10-5-0.998
Specific surface area range >0.0005 m2/g;标准样品测试重复性(RSD)≤1.0%
Pore size range 0.35nm-500nm;准确分析介孔和大孔,孔径重复性(SD)≤0.2nm
Pore volume range >0.0001 cm3/g
Degassing station 标准外置4站真空除气器
Degassing temperature ambient—400℃,控制精度1℃
Vacuum pump 两级旋片式机械真空泵,最终真空度6.7*10-2Pa
Physical Environmental temperature requirements L 510mm × W 530mm × H 930mm,重约40Kg
Environmental humidity requirements 15-35℃,20%-80%,无冷凝湿度
Power requirements 100-240VAC,50/60HZ,最大功率300W
Recommended applications 电池正负极材料、淀粉等制药辅料、炭黑、白炭黑、二氧化钛等多孔粉末、氧化铝、分子筛等催化材料、活性炭、沸石等吸附材料。
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3P graviSorb https://english.jwgb.net/3p-gravisorb.html https://english.jwgb.net/3p-gravisorb.html#respond Thu, 21 Dec 2023 07:56:00 +0000 https://english.jwgb.net/?p=475 https://english.jwgb.net/3p-gravisorb.html/feed 0 RuboLab MSB https://english.jwgb.net/rubolab-msb.html https://english.jwgb.net/rubolab-msb.html#respond Thu, 21 Dec 2023 07:53:44 +0000 https://english.jwgb.net/?p=473

Outline

Accurately determining the mass of lightweight samples is very important in many fields of research. In order to accomplish this, high-resolution analytical balances are an integral piece of equipment. Additionally, many technically relevant processes occur under technically demanding conditions such as high pressure, extreme temperatures, and aggressive or toxic atmospheres. Commercially available analytical balances cannot be used under these conditions. Therefore, the technology of the Magnetic Suspension Balance has been developed. RuboSORP´s Magnetic Suspension Balance technology offers the unique possibility of high-quality analysis under even the most extreme metrological conditions.

Availabe Versions

Version Type Max Pressure(bar) Temperature°C Resolution(ug) Max Load(g)
RuboSORP-150 150 -10-400 10 20
RuboSORP-150-HR 150 -10-400 1 10
RuboSORP-350 350 -10-200 10 20
RuboSORP-350-HR 350 -10-200 1 10
RuboSORP-700 700 -10-150 10 20
RuboSORP-700-HR 700 -10-150 1 10

The RuboLab Magnetic Suspension Balances (MSB) systems are available in 6 different versions, making them versatile for various pressure, temperature, and harsh chemistry conditions. The unique technology ensures measurements within a pressure range from vacuum to 700 bar and temperatures from -196C to 400°C. The measurement cell and all components in contact with process fluid are resistant to aggressive and toxic atmospheres. Due to this, a variety of different fluids can be used, e.g. inert gas, aggressive and toxic gases, supercritical fluids, flammable and combustible gases, gas mixtures, and vapor.

Measurement Technology

Magnetic Suspension Balance technology allows high resolution mass determination under extreme conditions. An industrial microbalance is located outside the cell. Thanks to contactless magnetic suspension coupling, mass changes within the pressurized cell can be determined. When perfroming a measurement, the sample whose mass change is being measured is attached to a permanent magnet. The actual position is detected and controlled via a high-performance PID controller. In order to establish a free levitation position for permanent magnet and measurement object, voltage is applied to a electromagnet outside of the measurement cell. This allows the sample mass to be measured contact free under extrem conditions. Load decoupling allows the object weight being measured to be substracted for taring or calibrating the measurement signal. In this case, only the permanent magnet remains in levitation position (zero-point position). When measuring point is selected, the measurement object is liftet, corresponding weight is detected by the microbalance. The measurement objects can be a crucible, containing sample material, for example being used to measure adsorption isotherms or catalytic reactions. In addition, the measurement object could also be sinker with calibrated volume for high accurate density measurement of the sinker surrounding fluid. The RuboSORP Magnetic Suspension Balance is an advanced technology for measuring the mass of two measurement objects at the same time.

Highlights

Simultaneous Measurement of two Samples

The Magnetic Suspension Balance can simultaneously measure two different sample materials or sinker (Dual sample version).

Forced Flow Through Measurement Conditions

The Magnetic Suspension Balance can be equipped with a forced flow though sample crucible which improves interaction between sample and surrounding fluid atmosphere.

Most Advanced Magnetic Suspension Balance Technology

The Balance is equipped with unique features, e.g. a self-optimizing Magnetic Suspension Balance controller as well as a failsafe high speed ethernet interface.

Integrated Calculation of Measurement Uncertainty

The software which will be used for controlling RuboSORP Magnetic Suspension Balance contains an integrated calculation of measurement uncertainy according to GUM guidelines (Guide to the expression of uncertainties in measurement). This allows a more holistic view of data and best level of scientific work.

Measurement Technology

Our Magnetic Suspension Balances are equipped with the latest generation of ultra-modern control electronics. In this way an even better, unrivalled measuring performance is achieved. The newly developed control system contains the specifications listed below:

- High-speed data transfer via Ethernet interface
- Exact approach of the measuring points without signal oscillations
- Online measured data display on the front display
- Failure minimization thanks to latest software application
- Integrated emergency power supply. In the event of a power failure, the Magnetic Suspension
- Balance is automatically set to a safe operating state. Uncontrollable operating states,
- which could lead to the crucible falling off, for example, are thus avoided.

Applications

Chlorine Gas Adsorption

The figure shows the experimental results of adsorption measurement using highly toxic chlorine gas. This data was collected simultaneously on two materials within a pressure range of up to 3.5 bar at 10°C. For this purpose, the Magnetic Suspension Balance has been equipped with two sample crucibles to measure both samples at the same time (dual sample measurement).

Adsorption of Biogas on Zeolite

With increasing usage of biogas as energy source, the corresponding purification treatment of its gas components has become increasingly more important. The figure shows the pure gas isotherms of CO2, CH4, N2 and H2 measured on zeolite, which is an industrially used sorbent for biogas purification. In combination with an appropriate dosing unit, the Magnetic Suspension Balance can also be used to measure the corresponding gas mixture adsorption.

Fluid Density Measurement

Sinkers with a known volume can be used instead of sample crucibles for high accurate determination of fluid phase density, even in supercritical atmospheres. The figure shows density data of CO2 measured in sub-critical and supercritical state. By using a sinker and sample crucible as measurement objects a combined measurement of adsorption and fluid density can be obtained.

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Prep J https://english.jwgb.net/prep-j.html https://english.jwgb.net/prep-j.html#respond Thu, 21 Dec 2023 07:51:13 +0000 https://english.jwgb.net/?p=471

Outline

Physical: 405mm*360mm*700mm, weight: 20kg Power:110/220V±20V, 50/60Hz, maximum power: 300w

Distinctive

  • Degassing temperature
  • Ambient~400℃
    Control accuracy: ±1℃, Each degassing position can control temperature independently.Intuitive and clear digital tube display.
  • Datasheet
  • Powder elutriation control
  • Each degassing position is equipped with an independent powder elutriation control unit,and integrated design with chuck.The filter element is made of acetate fiber material.Filter length up to 15mm, which effectively prevent the contamination of the system by powder samples.
  • Datasheet
  • Vacuum pump
  • Two-stage rotary vane type mechanical vacuum pump , with ultimate vacuum to 10-2Pa
  • Datasheet
  • Heating mantle
  • Using high-grade thermal insulation cotton liner,External soft packing material,built-in thermocouple,easier to wrap the sample tube, make the heating temperature more uniform.
  • Datasheet
  • Compatibility
  • Fully compatible with micromeritics sample tube (1/2"3/8"1/4"), Anton-Paar sample tube (12mm 9mm 6mm),to achieve the universality of the equipment. Chuck adopts the tower structure design.
  • Datasheet
  • Pressure display
  • Real-time display of the pressure in the sample tube, intuitively judge whether the vacuum degree meets the standard
  • Datasheet
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Vapor 100 https://english.jwgb.net/vapor-100.html https://english.jwgb.net/vapor-100.html#respond Mon, 18 Dec 2023 07:43:59 +0000 https://english.jwgb.net/?p=454

Outline

Parts Vapor 200C Vapor 100C Vapor 100B
Evaporators 1 1 1
Vapor Sorption Station 1 (1/0.1 Torr) 1 (1/0.1 Torr) 1 (10 Torr)
Micropore Analysis Station 1 (1/0.1 Torr) NO NO
Pressure Sensors 7 5 4
Cold Trap 1 2 2
Preparation Bit NO
( Can be prepared in situ)
1 1
Thermostatic Water Bath 1 (0 - 50 oC) 1 (0 - 50 oC) 1 (0 - 50 oC)
Dewar flask (1L) 2 NO NO
Dewar flask (3L) 1 2 2
Mechanical Pump One corrosion-resisting pump One corrosion-resisting pump,and One mechanical pump One corrosion-resisting pump(or One mechanical pump)
Molecular Pump 1 1 NO

Features

  • Preparation of adsorbate by evaporator.
  • Use stainless steel and thermostatic control module as manifold.
    Constant temperature range: room temperature to 50 oC.
  • Effective cold trap system prevents vapor from polluting vacuum
    pump and environment.
  • FFKM (Perfluoroelastomer) O rings for banner sealing
    performance.

Applications

  • Measurements of BET surface area and pore size distribution.
  • Measurements of various gas and steam adsorption isotherms.
  • Testing of isosteric heat of adsorption.
  • Determination of selective adsorption coefficient.

Main Parameters

Parts Vapor 200C Vapor 100C Vapor 100B
Testing Principle The static volumetric method
Data Features BET surface area: ≥ 0.01 m2/g
Mesopore: 2 - 500 nm (BJH)
Micropore: 0.35 - 2 nm (t-plot, DR, MP,DA, HK ,SF)
Physical Adsorbate N2, Ar, Kr, CO2
Vapor Adsorbate Carbon monoxide, ammonia, and a substance that is liquid at
room temperature.(Except corrosive, hyper-toxic, hazardous gas)
Same as Vapor 200C and Vapor 100C,
but p0 is greater than 1KPa
Physical Adsorption
Temperature
77K, 87K
Vapor Adsorption Temperature 0 - 50 oC
Steam Recovery Cold trap in analysis station Double cold trap in analysis and pretreatment station
Pretreatment Vacuum in-situ pretreatment Separate preposition and vacuum in-situ pretreatment

Essential Parameters

Evaporator Phase of adsobate transforming from liquid to gas by evaporator in room temperature,
implements test requirements
Adsorption Pressure P/P0 is less than 1 (P0 is saturated vapor pressure of
adsobate in adsorption temperature)
Vacuum Pump Special corrosion – resistant two stage rotary vane vacuum pump, molecular pump
Pressure Sensor 1000 Torr, 10 Torr, 1Torr
Sorption Temperature -196 oC is provided by liquid nitrogen in low temperature Dewar flask;
0 - 50 oC is provided by thermostatic water bath.
Number of Gas Inlet Providing separate gas intakes according to customer requirements. (Number of
intakes is multiples of 4).
Gas Recovery Effective cold trap system prevents from polluting vacuum pump and environment by
vapor.
Pretreatment Vacuum in –situ pretreatment, temperature ≤400 oC ±1 oC.

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Meso 400 https://english.jwgb.net/meso-400.html https://english.jwgb.net/meso-400.html#respond Mon, 18 Dec 2023 07:29:22 +0000 https://english.jwgb.net/?p=445

Outline

The Meso 400 is a compact sorption analyzer with four completely independent analysis stations for the determination of BET surface area, total pore volume and pore size distributions of mesoporous and macroporous materials. Each analysis station can be programmed individually and started at any given time. This is achieved by four independent dosing volumes and without any time loss. Next to Nitrogen, it is possible to employ any non-corrosive gas as an adsorbate such as CO2, Ar, Kr, H2, O2, CO, NH3 or CH4. All four analysis stations can also be used as in-situ degassing stations for sample preparation.

Features

  • Test Module
  • Internal temperature of test module can be controlled through Real-time monitoring, ensuring accuracy of adsorption detection.
  • Saturated Vapor Pressure P0
  • Using independent P0 pressure sensor for P0 value by inching test, guarantees the reliability of experimental data. Atmospheric pressure input method to determine P0 also be selected.
  • Datasheet
  • Vacuum System
  • It’s a multi-channel, adjustable, and parallel vacuum system. Vacuum degree of this system can be controlled in segments.
    This design prevents the sample from being pumped into analyzer. Meanwhile, a delicate part was designed for ensuring cleanliness of vacuum system, minimizing dust pollution.
  • JWGB Sample Preparation Device
  • It’s optional. External sample preparation device with four-degas stations in vacuum and heat to remove air from surface and pores of samples.
    Temperature can be set and monitored individually and controlled from ambient to 400 oC.
  • Pressure Sensor
  • A high-precision capacitive thin film pressure sensor, makes the partial pressure of P/P0 up to 10-4 (N2/77K) in the physical adsorption analysis.
  • Datasheet
  • Cold Free Space
  • Cold free space can be corrected by Helium automatically, ensuring accuracy of test results.
    This calibration method is suitable for testing of any powder or particle material.
  • Control of Liquid Nitrogen level
  • Using High volume (3L) Dewar flasks and working with the fixative seal cover assure a constant thermal profile along the length of sample tubes and P0 tubes throughout testing process.
  • Datasheet

Software

  • JWGB-BK Software is intelligent software in operation control, data acquisition, calculation and analysis and report generation on the Windows platform. This software can communicate with the host through the LAN port and remotely control many instruments at the same time.
  • Clear tabular reports include:
      Adsorption and desorption isotherms
      Single-/Multipoint BET surface area
      Langmuir surface area
      STSA-surface area
      pore size distribution according to BJH
      t-plot
      Dubinin-Radushkevich
      Horvath-Kawazoe
      Saito-Foley
  • Datasheet
  • Datasheet
  • JWGB-BK Software adopts a unique intake control method, the pressure in adsorption and desorption process is optimally set in six- stage; this flexible design is helpful for improving test efficiency.
  • Datasheet
  • Changes of the pressure and temperature inside the manifold can be observed directly in the test interface which is convenient for sample test and instrument maintenance.
    Current state of analyzer can be intuitively understood with the indicator light and event bar.
    Each adsorption equilibrium process is dynamically displayed on the test interface. Adsorption characteristics of the sample can be easily understood.
  • Datasheet

Case

  • BET repeatability is only 0.0015 m2 / g in the test of very low surface area powder
  • Datasheet Datasheet
  • Analysis value of pore size distribution in activated carbon materials as follows:
  • Datasheet Datasheet
  • Microporous analysis Report of carbon materials as below:
  • Datasheet Datasheet

Specification

FeatureMeso 400A
Adsorbed GasNon corrosive gases, such as N2, Ar, Kr, H2, O2, CO2, CO, NH3, CH4, etc.
Pressure Sensor at
Analysis Station
Accuracy: ±0.15% (F.S.)
Analysis StationEach analytical station is equipped with a pressure sensor.
Degas System The standard configuration is 4 stations in-situ degassing, which can simultaneously degas 4 samples with heating in vacuum; External sample preparation device with four-degas stations.
Degas TemperatureAmbient to 400 oC. Free to set up target temperature.
Cold Trap 1
Vacuum Pump Two-stage rotary vane mechanical vacuum pump, the ultimate pressure is 6.7*10-2 Pa.
Analysis Port Samples at four analysis ports can be tested at the same time.
Test Principle Gas adsorption by static-volumetric analysis
Measurement Range of
Specific Surface Area
0.0005 m2/g to the infinity;
Standard sample repetition is less than ± 1.0%.
Test Range of Pore Diameter Repeatability of pore size is less than 0.2 nm in the accurate analysis of porous materials which size is more than 2 nm.
Minimum Pore Volume 0.0001 cm3/g
Range of Relative Pressure P/P0 10-4-0.998
Overall Dimension Depth: 840 mm; width: 630 mm; height: 940 mm; weight: 85Kg
Ambient Temperature15-40 oC
Related Humidity30%-60%
Electrical SupplyAC220 V ± 20 V, 50/60 HZ, maximum power 300W;

Applications

Applied FieldTypical Materials Details
Material Researchceramic powder, metal powder, nanotubeAccording to surface area value of nanotube, hydrogen storage capacity can be predicted.
Chemical Engineeringcarbon black, amorphous silica, zinc oxide, titanium dioxideIntroduction of carbon black in rubber matrix can improve mechanical properties of rubber products. Surface area of carbon black is one of the important factors affecting the reinforcement performance of rubber products.
New Energylithium cobalt, lithium manganateIncreasing surface area of electrode can improve Electrochemical reaction rate and promote iron exchange in negative electrode.
Catalytic Technologiesactive alumina oxide, molecular sieve, zeoliteActive surface area and pore structure influence reaction rate.
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Micro 300 https://english.jwgb.net/micro-300.html https://english.jwgb.net/micro-300.html#respond Mon, 18 Dec 2023 07:19:09 +0000 https://english.jwgb.net/?p=443

Outline

The JWGB 300 Series can accurately produce surface area and pore size results of powder materials. According to the different test functions, this series of instruments are divided into three types, there are A, B, and C. Every analysis station has its own dedicated dosing manifold for optimal analysis duration. The C type is configured with 1 torr or 0.1 torr high-sensitive pressure sensors and turbo molecular pump with ultimate pressure of 10-8 Pa. The three analysis stations can also be used for in-situ sample preparation to avoid sample contamination. It can effectively take microporous analysis of microporous materials such as molecular sieve, catalyst, activated carbon, and other microporous materials.

Features

  • Test Module
  • Internal temperature of test module can be controlled through Real-time monitoring, ensuring accuracy of adsorption detection.
  • Saturated Vapor Pressure P0
  • Using independent P0 pressure sensor for P0 value by inching test, guarantees the reliability of experimental data. Atmospheric pressure input method to determine P0 also be selected.
  • Datasheet
  • Vacuum System
  • It’s a multi-channel, adjustable, and parallel vacuum system. Vacuum degree of this system can be controlled in segments. This design prevents the sample from being pumped into analyzer. Meanwhile, a delicate part was designed for ensuring cleanliness of vacuum system, minimizing dust pollution.
  • Sample Preparation System
  • In addition to external pretreatment devices, three analysis stations can be also used in preparing samples. Degas temperature can be set individually and controlled from ambient to 400 oC.
  • Micropore Distribution
  • Accurately apply the HK method, SF method and other micropore analysis model, the aperture deviation of micropore is less than 0.02 nm.
  • Pressure Sensor
  • Micro 300 with 1torr (selectable 0.1torr) makes the partial pressure of P/P0 up to 10-7 - 10-8 (N2/77K) in the physical adsorption analysis.
  • Datasheet
  • Cold Free Space
  • Cold free space can be corrected by Helium automatically, ensuring accuracy of test results.
    This calibration method is suitable for testing of any powder or particle material.
  • Control of Liquid Nitrogen level
  • Using High volume (3L) Dewar flasks and working with the seal cover assure a constant thermal profile along the length of sample tubes and P0 tubes throughout testing process.
  • Turbo Molecular Pump
  • Molecular pump is a standard configuration part on the Micro 300. The ultimate pressure is up to 10-8 Pa, providing a strong support for micropore analysis in the ultra-low pressure. The smallest micropore diameter can be tested is 0.35 nm.

Software

  • JWGB-BK Software is intelligent software in operation control, data acquisition, calculation and analysis and report generation on the Windows platform. This software can communicate with the host through the LAN port and remotely control many instruments at the same time.
  • Clear tabular reports include:
      Adsorption and desorption isotherms
      Single-/Multipoint BET surface area
      Langmuir surface area
      STSA-surface area
      pore size distribution according to BJH
      t-plot
      Dubinin-Radushkevich
      Horvath-Kawazoe
      Saito-Foley
  • Datasheet
  • Datasheet
  • JWGB-BK Software adopts a unique intake control method, the pressure in adsorption and desorption process is optimally set in six- stage; this flexible design is helpful for improving test efficiency.
  • Datasheet
  • Changes of the pressure and temperature inside the manifold can be observed directly in the test interface which is convenient for sample test and instrument maintenance.
    Current state of analyzer can be intuitively understood with the indicator light and event bar.
    Each adsorption equilibrium process is dynamically displayed on the test interface. Adsorption characteristics of the sample can be easily understood.
  • Datasheet

Case

  • BET repeatability is only 0.0015 m2 / g in the test of very low surface area powder
  • Datasheet Datasheet
  • Analysis value of pore size distribution in activated carbon materials as follows:
  • Datasheet Datasheet
  • Microporous analysis Report of carbon materials as below:
  • Datasheet Datasheet

Specification

FeatureMeso 300A Micro 300BMicro 300C
Adsorbed GasNon corrosive gases, such as N2, Ar, Kr, H2, O2, CO2, CO, NH3, CH4, etc.
Pressure Sensor at
Analysis Station
1000 torr, 31000 torr, 3;
10 torr, 1 (optional 2 or 3);
1 torr(0.1torr can be selected),1 (optional 2 or 3)
1000 torr, 3;
10 torr, 3;
1 torr (0.1torr can be selected), 3
Accuracy: ±0.15% (F.S.)
Pressure Sensor at P0 Station1000 torr,3
(Accuracy: ±0.15% (F.S.)
Degas System The standard configuration is 3 stations in-situ degassing, which can simultaneously degas 3 samples under vacuum heating;
Another optional external 4-station vacuum heating degassing machine;
Degas TemperatureAmbient to 400 ℃. Free to set up target temperature.
Cold Trap 1
Vacuum Pump Two-stage rotary vane mechanical
vacuum pump,
the ultimate pressure is
6.7*10-2 Pa
Two-stage rotary vane mechanical
vacuum pump, the ultimate
pressure is 6.7*10-2 Pa, optional turbo
molecular pump
Turbo molecular pump (ultimate pressure 10-8 Pa) and front
mechanical vacuum pump
(ultimate pressure is 6.7*10-2 Pa)
Analysis Port Samples on the 3 analysis bits can be tested at same time (including P0 test).
Test Principle Gas adsorption by static-volumetric analysis
Measurement Range of
Specific Surface Area
0.0005 m2/g to the infinity;
Standard sample repeat accuracy is less than ± 1.0%
0.0001m2/g to the infinity;
Standard sample repeat accuracy is less than ± 1.0%
0.0001m2/g to the infinity;
Standard sample repeat accuracy is less than ± 1.0%
Test Range of Pore Diameter 0.35 nm-500 nm; Pore dimension repeatability is less than 0.2 nm in the accurate analysis of materials with pore size greater than 2 nm 0.35 nm-500 nm; Pore dimension repeatability is less than 0.02 nm in the accurate analysis of micropore 0.35 nm-2 nm 0.35 nm-500 nm; Pore dimension repeatability is less than 0.02 nm in the accurate analysis of micropore 0.35 nm-2 nm
Minimum Pore Volume 0.0001 cm3/g
Range of Relative Pressure P/P0 10-5-0.99810-6/10-8-0.998 10-8-0.998
Overall Dimension Depth: 870 mm; width: 570 mm; height: 890 mm; weight: 80 Kg -90 Kg
Ambient Temperature15-40 oC
Related Humidity30%-60%
Electrical SupplyAC220 V ± 20 V, 50/60 HZ, maximum power 300W;

Specification

Applied FieldTypical Materials Details
Material Researchceramic powder, metal powder, nanotubeAccording to surface area value of nanotube, hydrogen storage capacity can be predicted.
Chemical Engineeringcarbon black, amorphous silica, zinc oxide, titanium dioxideIntroduction of carbon black in rubber matrix can improve mechanical properties of rubber products. Surface area of carbon black is one of the important factors affecting the reinforcement performance of rubber products.
New Energylithium cobalt, lithium manganateIncreasing surface area of electrode can improve Electrochemical reaction rate and promote iron exchange in negative electrode.
Catalytic Technologiesactive alumina oxide, molecular sieve, zeoliteActive surface area and pore structure influence reaction rate.
]]>
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Micro 200 https://english.jwgb.net/micro-200.html https://english.jwgb.net/micro-200.html#respond Mon, 18 Dec 2023 07:04:00 +0000 https://english.jwgb.net/?p=440

Outline

The JWGB 200 Series can accurately produce surface area and pore size results of powder materials. According to the different test functions, this series of instruments are divided into three types, there are A, B, and C, the C type is configured with 1 torr or 0.1 torr high-sensitive pressure sensors and turbo molecular pump with ultimate pressure of 10-8 Pa, it can effectively take microporous analysis of microporous materials such as molecular sieve, catalyst, activated carbon, and other microporous materials.

Features

  • Test Module
  • Internal temperature of test module can be controlled through Real-time monitoring, ensuring accuracy of adsorption detection.
  • Saturated Vapor Pressure P0
  • Using independent P0 pressure sensor for P0 value by inching test, guarantees the reliability of experimental data. Atmospheric pressure input method to determine P0 also be selected.
  • Datasheet
  • Vacuum System
  • It’s a multi-channel, adjustable, and parallel vacuum system. Vacuum degree of this system can be controlled in segments.
    This design prevents the sample from being pumped into analyzer. Meanwhile, a delicate part was designed for ensuring cleanliness of vacuum system, minimizing dust pollution.
  • Sample Preparation System
  • In addition to two pretreatment stations, the other two analysis stations can be used in preparing samples. There is no interference between pretreatment stations and analysis stations. Degas temperature can be set individually and controlled from ambient to 400 ℃.
  • Micropore Distribution
  • Accurately apply the HK method, SF method and other micropore analysis model, the aperture deviation of micropore is less than 0.02 nm.
  • Pressure Sensor
  • Micro 200C with 1torr (selectable 0.1torr) makes the partial pressure of P/P0 up to 10-7 - 10-8 (N2/77K) in the physical adsorption analysis.
  • Datasheet
  • Cold Free Space
  • Cold free space can be corrected by Helium automatically, ensuring accuracy of test results.
    This calibration method is suitable for testing of any powder or particle material.
  • Control of Liquid Nitrogen level
  • Using High volume (3L) Dewar flasks and working with the seal cover assure a constant thermal profile along the length of sample tubes and P0 tubes throughout testing process.
  • Turbo Molecular Pump
  • Molecular pump is a standard configuration part on the Micro 200C. The ultimate pressure is up to 10-8 Pa, providing a strong support for micropore analysis in the ultra-low pressure. The smallest micro-pore diameter can be tested is 0.35 nm.

Software

  • JWGB-BK Software is intelligent software in operation control, data acquisition, calculation and analysis and report generation on the Windows platform. This software can communicate with the host through the LAN port and remotely control many instruments at the same time.
  • Clear tabular reports include:
      Adsorption and desorption isotherms
      Single-/Multipoint BET surface area
      Langmuir surface area
      STSA-surface area
      pore size distribution according to BJH
      t-plot
      Dubinin-Radushkevich
      Horvath-Kawazoe
      Saito-Foley
  • Datasheet
  • Datasheet
  • JWGB-BK Software adopts a unique intake control method, the pressure in adsorption and desorption process is optimally set in six- stage; this flexible design is helpful for improving test efficiency.
  • Datasheet
  • Changes of the pressure and temperature inside the manifold can be observed directly in the test interface which is convenient for sample test and instrument maintenance.
    Current state of analyzer can be intuitively understood with the indicator light and event bar.
    Each adsorption equilibrium process is dynamically displayed on the test interface. Adsorption characteristics of the sample can be easily understood.
  • Datasheet

Case

  • BET repeatability is only 0.0015 m2 / g in the test of very low surface area powder
  • Datasheet Datasheet
  • Analysis value of pore size distribution in activated carbon materials as follows:
  • Datasheet Datasheet
  • Microporous analysis Report of carbon materials as below:
  • Datasheet Datasheet

Specification

Feature Meso 200A Micro 200B Micro 200C
Adsorbed Gas Non corrosive gases, such as N2, Ar, Kr, H2, O2, CO2, CO, NH3, CH4, etc.
Pressure Sensor at
Analysis Station
1000 torr, 2 1000 torr, 2;
10 torr, 1 (optional 2);
1 torr(0.1torr can be selected), optional 1
1000 torr, 2;
10 torr, 2;
1 torr (0.1torr can be selected), 2
Accuracy: ±0.15% (F.S.)
Pressure Sensor at P0 Station 1000 torr,2
(Accuracy: ±0.15% (F.S.)
Degas System Two ectopic sample preparation ports;
(Analysis station supports in situ sample preparation)
Degas Temperature Ambient to 400 ℃. Free to set up target temperature.
Cold Trap 1
Vacuum Pump Two-stage rotary vane mechanical
vacuum pump,
the ultimate pressure is
6.7*10-2 Pa
Two-stage rotary vane mechanical
vacuum pump, the ultimate
pressure is 6.7*10-2 Pa, optional
turbo molecular pump
Turbo molecular pump (ultimate pressure 10-8 Pa) and front
mechanical vacuum pump
(ultimate pressure is 6.7*10-2 Pa)
Analysis Port Samples on the 2 analysis bits can be tested alternately (including P0 test).
Test Principle Gas adsorption by static-volumetric analysis
Measurement Range of
Specific Surface Area
0.0005 m2/g to the infinity;
Standard sample repeat accuracy is less than ± 1.0%
0.0001m2/g to the infinity;
Standard sample repeat accuracy is less than ± 1.0%
0.0001m2/g to the infinity;
Standard sample repeat accuracy is less than ± 1.0%
Test Range of Pore Diameter 0.35 nm-500 nm; Pore dimension repeatability is less than 0.2 nm in the accurate analysis of materials with pore size greater than 2 nm 0.35 nm-500 nm; Pore dimension repeatability is less than 0.02 nm in the accurate analysis of micropore 0.35 nm-2 nm 0.35 nm-500 nm; Pore dimension repeatability is less than 0.02 nm in the accurate analysis of micropore 0.35 nm-2 nm
Minimum Pore Volume 0.0001 cm3/g
Range of Relative Pressure P/P0 10-5-0.998 10-6/10-8-0.998 10-8-0.998
Overall Dimension Depth: 870 mm; width: 570 mm; height: 890 mm; weight: 80 Kg -90 Kg
Ambient Temperature 15-40 oC
Related Humidity 30%-60%
Electrical Supply AC220 V ± 20 V, 50/60 HZ, maximum power 300W;

Specification

Applied Field Typical Materials Details
Material Research ceramic powder, metal powder, nanotube According to surface area value of nanotube, hydrogen storage capacity can be predicted.
Chemical Engineering carbon black, amorphous silica, zinc oxide, titanium dioxide Introduction of carbon black in rubber matrix can improve mechanical properties of rubber products. Surface area of carbon black is one of the important factors affecting the reinforcement performance of rubber products.
New Energy lithium cobalt, lithium manganate Increasing surface area of electrode can improve Electrochemical reaction rate and promote iron exchange in negative electrode.
Catalytic Technologies active alumina oxide, molecular sieve, zeolite Active surface area and pore structure influence reaction rate.
]]>
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Micro 100 https://english.jwgb.net/micro-100.html https://english.jwgb.net/micro-100.html#respond Mon, 18 Dec 2023 06:30:32 +0000 https://english.jwgb.net/?p=438

Outline

The JWGB 100 Series can accurately produce surface area and pore size results of powder materials. According to the different test functions, this series of instruments are divided into three types, there are A, B, and C, the C type is configured with 1 torr or 0.1 torr high-sensitive pressure sensors and turbo molecular pump with ultimate pressure of 10-8 Pa, it can effectively take microporous analysis of microporous materials such as molecular sieve, catalyst, activated carbon, and other microporous materials.

Features

  • Test Module
  • Internal temperature of test module can be controlled through Real-time monitoring, ensuring accuracy of adsorption detection.
  • Saturated Vapor Pressure P0
  • Using independent P0 pressure sensor for P0 value by inching test, guarantees the reliability of experimental data. Atmospheric pressure input method to determine P0 also be selected.
  • Datasheet
  • Vacuum System
  • It’s a multi-channel, adjustable, and parallel vacuum system. Vacuum degree of this system can be controlled in segments. This design prevents the sample from being pumped into analyzer. Meanwhile, a delicate part was designed for ensuring cleanliness of vacuum system, minimizing dust pollution.
  • Sample Preparation System
  • In addition to two pretreatment stations, the other two analysis stations can be used in preparing samples. There is no interference between pretreatment stations and analysis stations. Degas temperature can be set individually and controlled from ambient to 400 ℃.
  • Micropore Distribution
  • Accurately apply the HK method, SF method and other micropore analysis model, the aperture deviation of micropore is less than 0.02 nm.
  • Pressure Sensor
  • Micro 100C with 1torr (selectable 0.1torr) makes the partial pressure of P/P0 up to 10-7 - 10-8 (N2/77K) in the physical adsorption analysis.
  • Datasheet
  • Cold Free Space
  • Cold free space can be corrected by Helium automatically, ensuring accuracy of test results.
    This calibration method is suitable for testing of any powder or particle material.
  • Control of Liquid Nitrogen level
  • Using High volume (3L) Dewar flasks and working with the seal cover assure a constant thermal profile along the length of sample tubes and P0 tubes throughout testing process.
  • Turbo Molecular Pump
  • Molecular pump is a standard configuration part on the Micro 100C. The ultimate pressure is up to 10-8 Pa, providing a strong support for micropore analysis in the ultra-low pressure. The smallest micro-pore diameter can be tested is 0.35 nm.

Software

  • JWGB-BK Software is intelligent software in operation control, data acquisition, calculation and analysis and report generation on the Windows platform. This software can communicate with the host through the LAN port and remotely control many instruments at the same time.
  • Clear tabular reports include:
      Adsorption and desorption isotherms
      Single-/Multipoint BET surface area
      Langmuir surface area
      STSA-surface area
      pore size distribution according to BJH
      t-plot
      Dubinin-Radushkevich
      Horvath-Kawazoe
      Saito-Foley
  • Datasheet
  • Datasheet
  • JWGB-BK Software adopts a unique intake control method, the pressure in adsorption and desorption process is optimally set in six- stage; this flexible design is helpful for improving test efficiency.
  • Datasheet
  • Changes of the pressure and temperature inside the manifold can be observed directly in the test interface which is convenient for sample test and instrument maintenance.
    Current state of analyzer can be intuitively understood with the indicator light and event bar.
    Each adsorption equilibrium process is dynamically displayed on the test interface. Adsorption characteristics of the sample can be easily understood.
  • Datasheet

Case

  • BET repeatability is only 0.0015 m2 / g in the test of very low surface area powder
  • Datasheet Datasheet
  • Analysis value of pore size distribution in activated carbon materials as follows:
  • Datasheet Datasheet
  • Microporous analysis Report of carbon materials as below:
  • Datasheet Datasheet

Specification

FeatureMeso 100A Micro 100BMicro 100C
Adsorbed GasNon corrosive gases, such as N2, Ar, Kr, H2, O2, CO2, CO, NH3, CH4, etc.
Pressure Sensor at
Analysis Station
1000 torr1000 torr,10 torr 1000 torr,
10 torr, 1 torr (optional 0.1 torr)
Accuracy: ±0.15% (F.S.)
Pressure Sensor at P0 Station1000 torr
(Accuracy: ±0.15% (F.S.)
Degas System 2 ectopic vacuum heating degas station;
Samples on analysis bits can be degassed simutaneously.
Degas TemperatureAmbient to 400 ℃. Free to set up target temperature.
Cold Trap 1
Vacuum Pump Two-stage rotary vane mechanical vacuum pump,
the trtimate vacuum is 6.7*10-2 Pa
Turbo molecular pump (trtimate vacuum 10-8 Pa) and front mechanical vacuum pump
Analysis Port Samples on the 2 analysis bits can be tested alternately (including P0 test).
Test Principle Gas adsorption by static-volumetric analysis
Measurement Range of
Specific Surface Area
0.0005 m2/g to the infinity;
Standard sample repetition is less than ± 1.0%
Test Range of Pore 0.35 nm-500 nm; 0.35 nm-500 nm; 0.35 nm-500 nm;
Diameter repeatability of pore size is less
than 0.2 nm in the accurate
analysis of porous materials
which size is more than 2 nm
repeatability of pore size is less
than 0.2 nm in the accurate
analysis 0.7 nm-2 nm micropore.
repeatability of pore size is less
than 0.2 nm in the accurate
analysis 0.35 nm-2 nm micropore.
Range of Relative Pressure P/P0 10-5-0.99810-6-0.998 10-8-0.998
Minimum Pore Volume 0.0001 cm3/g
Overall Dimension Depth: 870 mm; width: 570 mm; height: 890 mm; weight: 80 Kg -90 Kg
Ambient Temperature15-40 oC
Related Humidity30%-60%
Electrical SupplyAC220 V ± 20 V, 50/60 HZ, maximum power 300W;

Specification

Applied FieldTypical Materials Details
Material Researchceramic powder, metal powder, nanotubeAccording to surface area value of nanotube, hydrogen storage capacity can be predicted.
Chemical Engineeringcarbon black, amorphous silica, zinc oxide, titanium dioxideIntroduction of carbon black in rubber matrix can improve mechanical properties of rubber products. Surface area of carbon black is one of the important factors affecting the reinforcement performance of rubber products.
New Energylithium cobalt, lithium manganateIncreasing surface area of electrode can improve Electrochemical reaction rate and promote iron exchange in negative electrode.
Catalytic Technologiesactive alumina oxide, molecular sieve, zeoliteActive surface area and pore structure influence reaction rate.
]]>
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